%0 Journal Article %1 WOS:000241363300011 %A Meneses, C T %A Flores, W H %A Sotero, A P %A Tamura, E %A Garcia, F %A Sasaki, J M %C 2 ABBEY SQ, CHESTER, CH1 2HU, ENGLAND %D 2006 %I INT UNION CRYSTALLOGRAPHY %J JOURNAL OF SYNCHROTRON RADIATION %K XAS; in nanoparticles} situ {instrumentation; %N 6 %P 468-470 %R 10.1107/S0909049506033802 %T In situ system for X-ray absorption spectroscopy experiments to investigate nanoparticle crystallization %V 13 %X A new furnace, based on a halogen lamp, and a sample cell have been designed and constructed for in situ X-ray absorption spectroscopy experiments in conventional and dispersive mode ( transmission and fluorescence geometries). The main application of the apparatus is thermal treatment studies under controlled conditions for dynamical processes. The sol - gel ( gelatin) method has been utilized to synthesize NiO nanoparticles. During this heating process, in situ Ni K-edge X-ray absorption near-edge structural measurements provided evidence of the evolution of a Ni environment until complete NiO nanoparticle crystallization. This case is reported in order to show the furnace performance in dispersive mode.

@article{WOS:000241363300011, abstract = {A new furnace, based on a halogen lamp, and a sample cell have been designed and constructed for in situ X-ray absorption spectroscopy experiments in conventional and dispersive mode ( transmission and fluorescence geometries). The main application of the apparatus is thermal treatment studies under controlled conditions for dynamical processes. The sol - gel ( gelatin) method has been utilized to synthesize NiO nanoparticles. During this heating process, in situ Ni K-edge X-ray absorption near-edge structural measurements provided evidence of the evolution of a Ni environment until complete NiO nanoparticle crystallization. This case is reported in order to show the furnace performance in dispersive mode.}, added-at = {2022-05-23T20:00:14.000+0200}, address = {2 ABBEY SQ, CHESTER, CH1 2HU, ENGLAND}, author = {Meneses, C T and Flores, W H and Sotero, A P and Tamura, E and Garcia, F and Sasaki, J M}, biburl = {https://www.bibsonomy.org/bibtex/2a6de20b96cfce06cb46eb9204d4a6eaf/ppgfis_ufc_br}, doi = {10.1107/S0909049506033802}, interhash = {098b9c4cb4e236e1b2690f84bcb51cac}, intrahash = {a6de20b96cfce06cb46eb9204d4a6eaf}, issn = {1600-5775}, journal = {JOURNAL OF SYNCHROTRON RADIATION}, keywords = {XAS; in nanoparticles} situ {instrumentation;}, number = 6, pages = {468-470}, publisher = {INT UNION CRYSTALLOGRAPHY}, pubstate = {published}, timestamp = {2022-05-23T20:00:14.000+0200}, title = {In situ system for X-ray absorption spectroscopy experiments to investigate nanoparticle crystallization}, tppubtype = {article}, volume = 13, year = 2006 }