%0 Journal Article %1 wu_strip-shield_2009 %A Wu, Chin H %A Grant, Christopher V %A Cook, Gabriel A %A Park, Sang Ho %A Opella, Stanley J %D 2009 %J J. Magn. Reson. %K Biopolymers,Carbon Design,Hydrogen,Magnetic Fields,Equipment Interaction Isotopes,Computer Isotopes,Polytetrafluoroethylene,Protein Mapping,Proteins,Viral Proteins Resonance Simulation,Electromagnetic Spectroscopy,Nitrogen %N 1 %P 74--80 %R 10.1016/j.jmr.2009.06.004 %T A strip-shield improves the efficiency of a solenoid coil in probes for high-field solid-state \NMR\ of lossy biological samples %V 200 %X A strip-shield inserted between a high inductance double-tuned solenoid coil and the glass tube containing the sample improves the efficiency of probes used for high-field solid-state NMR experiments on lossy aqueous samples of proteins and other biopolymers. A strip-shield is a coil liner consisting of thin copper strips layered on a PTFE (polytetrafluoroethylene) insulator. With lossy samples, the shift in tuning frequency is smaller, the reduction in Q, and RF-induced heating are all significantly reduced when the strip-shield is present. The performance of 800MHz (1)H/(15)N and (1)H/(13)C double-resonance probes is demonstrated on aqueous samples of membrane proteins in phospholipid bilayers.

@article{wu_strip-shield_2009, abstract = {A strip-shield inserted between a high inductance double-tuned solenoid coil and the glass tube containing the sample improves the efficiency of probes used for high-field solid-state NMR experiments on lossy aqueous samples of proteins and other biopolymers. A strip-shield is a coil liner consisting of thin copper strips layered on a PTFE (polytetrafluoroethylene) insulator. With lossy samples, the shift in tuning frequency is smaller, the reduction in Q, and RF-induced heating are all significantly reduced when the strip-shield is present. The performance of 800MHz (1)H/(15)N and (1)H/(13)C double-resonance probes is demonstrated on aqueous samples of membrane proteins in phospholipid bilayers.}, added-at = {2017-03-14T02:48:56.000+0100}, author = {Wu, Chin H and Grant, Christopher V and Cook, Gabriel A and Park, Sang Ho and Opella, Stanley J}, biburl = {https://www.bibsonomy.org/bibtex/2ca6c6a636b842fdd6a3c18329764864c/nmrresource}, doi = {10.1016/j.jmr.2009.06.004}, interhash = {0ad73b798b3a0cf69c52bc48e89b918f}, intrahash = {ca6c6a636b842fdd6a3c18329764864c}, issn = {1096-0856}, journal = {J. Magn. Reson.}, keywords = {Biopolymers,Carbon Design,Hydrogen,Magnetic Fields,Equipment Interaction Isotopes,Computer Isotopes,Polytetrafluoroethylene,Protein Mapping,Proteins,Viral Proteins Resonance Simulation,Electromagnetic Spectroscopy,Nitrogen}, month = sep, number = 1, pages = {74--80}, pmid = {19559634}, timestamp = {2017-03-14T02:49:21.000+0100}, title = {{A strip-shield improves the efficiency of a solenoid coil in probes for high-field solid-state {\{}NMR{\}} of lossy biological samples}}, volume = 200, year = 2009 }