Article,

Synthesis and characterization of NiAl2O4 nanoparticles obtained through gelatin

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MATERIALS LETTERS, 61 (25): 4743-4746 (2007)
DOI: 10.1016/j.matlet.2007.03.042

Abstract

Nanoparticles of NiAl2O4 were synthesized by heating (500-1000 degrees C) the dried resin resultant of a mixture in aqueous solution of gelatin, NiCl2 center dot 6H(2)O and AlCl3 center dot 6H(2)O. The particle size and microstrain were calculated from the line broadening of X-ray powder diffraction peaks through the Rietveld method refinement: these are 3.9-16 mn and -0.743-0.139%, respectively. The NiAl2O4 nanoparticles were characterized by X-ray powder diffraction (XRPD), thermo gravimetric analysis (TG), BET and TEM techniques. (c) 2007 Elsevier B.V All rights reserved.

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