Two-dimensional chemical shift/heteronuclear dipolar coupling spectra obtained with polarization inversion spin exchange at the magic angle and magic-angle sample spinning (\PISEMAMAS\)
High-resolution two-dimensional 15N chemical shift/1H-15N dipolar coupling polarization inversion spin exchange at the magic angle (PISEMA) spectra of a polycrystalline sample of 15N-acetylvaline were obtained with and without magic-angle sample spinning. These spectra demonstrate the advantages of the PISEMA experiment over conventional approaches to separated local-field spectroscopy, especially the high resolution in the dipolar dimension where the spinning sidebands have uniformly narrow linewidths.
%0 Journal Article
%1 ramamoorthy_two-dimensional_1995
%A Ramamoorthy, A
%A Opella, S J
%D 1995
%J Solid State Nucl Magn Reson
%K Crystallization,Electron Resonance Spectroscopy,Magnetic Spectroscopy,Valine Spin
%N 6
%P 387--392
%T Two-dimensional chemical shift/heteronuclear dipolar coupling spectra obtained with polarization inversion spin exchange at the magic angle and magic-angle sample spinning (\PISEMAMAS\)
%V 4
%X High-resolution two-dimensional 15N chemical shift/1H-15N dipolar coupling polarization inversion spin exchange at the magic angle (PISEMA) spectra of a polycrystalline sample of 15N-acetylvaline were obtained with and without magic-angle sample spinning. These spectra demonstrate the advantages of the PISEMA experiment over conventional approaches to separated local-field spectroscopy, especially the high resolution in the dipolar dimension where the spinning sidebands have uniformly narrow linewidths.
@article{ramamoorthy_two-dimensional_1995,
abstract = {High-resolution two-dimensional 15N chemical shift/1H-15N dipolar coupling polarization inversion spin exchange at the magic angle (PISEMA) spectra of a polycrystalline sample of 15N-acetylvaline were obtained with and without magic-angle sample spinning. These spectra demonstrate the advantages of the PISEMA experiment over conventional approaches to separated local-field spectroscopy, especially the high resolution in the dipolar dimension where the spinning sidebands have uniformly narrow linewidths.},
added-at = {2017-03-14T02:48:56.000+0100},
author = {Ramamoorthy, A and Opella, S J},
biburl = {https://www.bibsonomy.org/bibtex/20cf1d54fff9f5239bc77f97655d2aaeb/nmrresource},
interhash = {4b0f2d15f78db11ff802b3b3cf59516a},
intrahash = {0cf1d54fff9f5239bc77f97655d2aaeb},
issn = {0926-2040},
journal = {Solid State Nucl Magn Reson},
keywords = {Crystallization,Electron Resonance Spectroscopy,Magnetic Spectroscopy,Valine Spin},
month = aug,
number = 6,
pages = {387--392},
pmid = {8581437},
timestamp = {2017-03-14T02:49:21.000+0100},
title = {{Two-dimensional chemical shift/heteronuclear dipolar coupling spectra obtained with polarization inversion spin exchange at the magic angle and magic-angle sample spinning ({\{}PISEMAMAS{\}})}},
volume = 4,
year = 1995
}