%0 Journal Article %1 Schmidt2009 %A Schmidt, Martin U. %A Brühne, Stefan %A Wolf, Alexandra %A Rech, Anette %A Brüning, Jürgen %A Alig, Edith %A Fink, Lothar %A Buchsbaum, Christian %A Glinnemann, Jürgen %A van de Streek, Jacco %A Gozzo, Fabia %A Brunelli, Michela %A Stowasser, Frank %A Gorelik, Tatiana %A Mugnaioli, Enrico %A Kolb, Ute %D 2009 %I International Union of Crystallography %J Acta Cryst. B %K dthcrys pdf py213 xrpd %N 2 %P 189--199 %R 10.1107/s0108768109003759 %T Electron diffraction, X-ray powder diffraction and pair-distribution-function analyses to determine the crystal structures of Pigment Yellow 213, C23H21N5O9 %U http://dx.doi.org/10.1107/s0108768109003759 %V 65 %X The crystal structure of the nanocrystalline ? phase of Pigment Yellow 213 (P.Y. 213) was solved by a combination of single-crystal electron diffraction and X-ray powder diffraction, despite the poor crystallinity of the material. The molecules form an efficient dense packing, which explains the observed insolubility and weather fastness of the pigment. The pair-distribution function (PDF) of the ? phase is consistent with the determined crystal structure. The ? phase of P.Y. 213 shows even lower crystal quality, so extracting any structural information directly from the diffraction data is not possible. PDF analysis indicates the ? phase to have a columnar structure with a similar local structure as the ? phase and a domain size in column direction of approximately 4 nm.

@article{Schmidt2009, abstract = {{The crystal structure of the nanocrystalline ? phase of Pigment Yellow 213 (P.Y. 213) was solved by a combination of single-crystal electron diffraction and X-ray powder diffraction, despite the poor crystallinity of the material. The molecules form an efficient dense packing, which explains the observed insolubility and weather fastness of the pigment. The pair-distribution function (PDF) of the ? phase is consistent with the determined crystal structure. The ? phase of P.Y. 213 shows even lower crystal quality, so extracting any structural information directly from the diffraction data is not possible. PDF analysis indicates the ? phase to have a columnar structure with a similar local structure as the ? phase and a domain size in column direction of approximately 4 nm.}}, added-at = {2019-03-11T21:00:05.000+0100}, author = {Schmidt, Martin U. and Br\"{u}hne, Stefan and Wolf, Alexandra and Rech, Anette and Br\"{u}ning, J\"{u}rgen and Alig, Edith and Fink, Lothar and Buchsbaum, Christian and Glinnemann, J\"{u}rgen and van de Streek, Jacco and Gozzo, Fabia and Brunelli, Michela and Stowasser, Frank and Gorelik, Tatiana and Mugnaioli, Enrico and Kolb, Ute}, biburl = {https://www.bibsonomy.org/bibtex/2346ab84fb43471c14445da2b0a48856b/fairybasslet}, citeulike-article-id = {4182363}, citeulike-linkout-0 = {http://dx.doi.org/10.1107/s0108768109003759}, citeulike-linkout-1 = {http://scripts.iucr.org/cgi-bin/paper?S0108768109003759}, doi = {10.1107/s0108768109003759}, interhash = {600217d7802a79935fe9108c933751fa}, intrahash = {346ab84fb43471c14445da2b0a48856b}, issn = {urn:issn:0108-7681}, journal = {Acta Cryst. B}, keywords = {dthcrys pdf py213 xrpd}, month = apr, number = 2, pages = {189--199}, posted-at = {2012-10-03 11:12:11}, priority = {2}, publisher = {International Union of Crystallography}, timestamp = {2019-03-11T21:06:37.000+0100}, title = {{Electron diffraction, X-ray powder diffraction and pair-distribution-function analyses to determine the crystal structures of Pigment Yellow 213, C23H21N5O9}}, url = {http://dx.doi.org/10.1107/s0108768109003759}, volume = 65, year = 2009 }