Article,
Direct Synthesis of Cd3OSO4 Nano-particles From a New Three-dimensional Cadmium(II) Coordination Polymer Precursor
G. Shahverdizadeh, S. Masoudian, A. Soudi, F. Bigdeli, H. Monfared, A. Morsali, and H. Khavasi.JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS, 21 (1): 171-174 (March 2011)
DOI: {10.1007/s10904-010-9443-9}
Abstract
A new three-dimensional Cd(II) coordination polymer,
\Cd-3(3-pyc)(4)(NCS)(2)(H2O)(4)center dot 2H(2)O\ (n) (1); 3-Hpyc
= 3-pyridinecarboxylic acid, was prepared and characterized by elemental
analyses and IR spectroscopy. Compound 1 was structurally characterized
by single-crystal X-ray diffraction. The structural determination shows
that the compound is a new 3D coordination polymer has different
environments containing CdO5NS and CdO2N4 units. This polymeric
precursor has been used in the preparation of Cd3OSO4 nanoparticles by
thermolysis in oleic acid. The new nano-structure of Cd3OSO4 was
characterized by scanning electron microscopy and X-ray powder
diffraction. This study demonstrates that coordination polymers may be
suitable precursors to the preparation of desirable nanoscale materials.
- BibTeX key
- ISI:000287249700021
- entry type
- article
- address
- VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS
- year
- 2011
- month
- MAR
- journal
- JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS
- number
- 1
- pages
- 171-174
- publisher
- SPRINGER
- volume
- 21
- type
- Article
- author-email
- Shahverdizadeh@iaut.ac.it morsali\_a@modares.ac.ir
- research-areas
- Polymer Science
- language
- English
- funding-text
- This work was supported by Tabriz Azad University.
- funding-acknowledgement
- Tabriz Azad University
- times-cited
- 3
- cited-references
- Abu-Youssef MAM, 1999, INORG CHEM, V38, P5716, DOI 10.1021/ic990656x. AKHBARI K, 2010, COORD CHEM IN PRESS, P254. Alvarez HM, 2004, POLYHEDRON, V23, P617, DOI 10.1016/j.poly.2003.10.015. Aoyagi M, 1999, J AM CHEM SOC, V121, P7457, DOI 10.1021/ja991301f. Ashoka S, 2010, MATER LETT, V64, P173, DOI 10.1016/j.matlet.2009.10.036. Askanneiad A, 2008, MATER LETT, V62, P478, DOI 10.1016/j.matlet.2007.05.082. Askarinejad A, 2009, CHEM ENG J, V150, P569, DOI 10.1016/j.cej.2009.03.005. BUNN AG, 1992, INORG CHEM, V31, P1297, DOI 10.1021/ic00033a031. Caneschi A, 2001, ANGEW CHEM INT EDIT, V40, P1760, DOI 10.1002/1521-3773(20010504)40:9<1760::AID-ANIE17600>3.0.CO;2-U. FUJITA M, 1994, J AM CHEM SOC, V116, P1151, DOI 10.1021/ja00082a055. Janiak C, 1998, J PRAK CHEM-CHEM ZTG, V340, P181, DOI 10.1002/prac.19983400214. Janiak C, 1998, MAIN GROUP MET CHEM, V21, P33. Janiak C, 1997, COORDIN CHEM REV, V163, P107, DOI 10.1016/S0010-8545(97)00011-8. Jayakrishnan R, 2003, THIN SOLID FILMS, V440, P19, DOI 10.1016/S0040-6090(03)00811-3. LENARVOR N, 1995, J AM CHEM SOC, V117, P7129, DOI 10.1021/ja00132a013. Mahjoub A, 2003, J COORD CHEM, V56, P779, DOI 10.1080/0095897031000110600. Mahmoudi G, 2007, CRYSTENGCOMM, V9, P704, DOI 10.1039/b702569f. Morsali A, 2005, SOLID STATE SCI, V7, P1429, DOI 10.1016/j.solidstatesciences.2005.08.013. Morsali A, 2005, INORG CHEM COMMUN, V8, P460, DOI 10.1016/j.inoche.2005.02.006. Morsali A, 2004, INORG CHEM COMMUN, V7, P1184, DOI 10.1016/j.inoche.2004.09.003. Morsali A, 2009, INORG CHIM ACTA, V362, P3427, DOI 10.1016/j.ica.2009.03.040. Morsali A, 2009, COORDIN CHEM REV, V253, P1882, DOI 10.1016/j.ccr.2009.02.018. Nagaraju G, 2009, MATER LETT, V63, P492, DOI 10.1016/j.matlet.2008.11.032. Nakamoto K., 1997, INFRARED RAMAN SPECT. Pyykko P, 1997, CHEM REV, V97, P597, DOI 10.1021/cr940396v. Ristic M, 2004, MATER LETT, V58, P2494, DOI 10.1016/j.matlet.2004.03.016. Salunkhe RR, 2009, APPL SURF SCI, V255, P3923, DOI 10.1016/j.apsusc.2008.10.035. Shi WJ, 2007, INORG CHIM ACTA, V360, P588, DOI 10.1016/j.ica.2006.08.004. Singh N, 2006, MATER LETT, V60, P3492, DOI 10.1016/j.matlet.2006.03.054. Xiao HP, 2005, HELV CHIM ACTA, V88, P2543, DOI 10.1002/hlca.200590192.
- issn
- 1574-1443
- affiliation
- Shahverdizadeh, GH (Reprint Author), Islamic Azad Univ, Dept Appl Chem, Res Lab, Tabriz Branch, Tabriz, Iran. Shahverdizadeh, Gholam Hossein, Islamic Azad Univ, Dept Appl Chem, Res Lab, Tabriz Branch, Tabriz, Iran. Masoudian, Shahla; Soudi, Ali Akbar; Monfared, Hassan Hosseini, Zanjan Univ, Dept Chem, Zanjan, Iran. Bigdeli, Fahime, Payame Noor Univ, Dept Chem, Abhar, Iran. Morsali, Ali, Tarbiat Modares Univ, Dept Chem, Fac Sci, Tehran, Iran. Khavasi, Hamid Reza, Shahid Beheshti Univ, Dept Chem, Tehran, Iran.
- orcid-numbers
- Hosseini-Monfared, Hassan/0000-0001-9157-8198
- usage-count-since-2013
- 7
- doc-delivery-number
- 719ZJ
- web-of-science-categories
- Polymer Science
- usage-count-last-180-days
- 1
- number-of-cited-references
- 30
- journal-iso
- J. Inorg. Organomet. Polym. Mater.
- keywords-plus
- RAY CRYSTAL-STRUCTURE; COMPLEXES; CDO; CHEMISTRY; CD(OH)(2); LIGANDS; IONS
- unique-id
- ISI:000287249700021
- DOI
- 10.1007/s10904-010-9443-9
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%1 ISI:000287249700021
%A Shahverdizadeh, Gholam Hossein
%A Masoudian, Shahla
%A Soudi, Ali Akbar
%A Bigdeli, Fahime
%A Monfared, Hassan Hosseini
%A Morsali, Ali
%A Khavasi, Hamid Reza
%C VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS
%D 2011
%I SPRINGER
%J JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS
%K Cadmium(II)} Nano-materials; Thermal properties; structure; {Crystal
%N 1
%P 171-174
%R 10.1007/s10904-010-9443-9
%T Direct Synthesis of Cd3OSO4 Nano-particles From a New Three-dimensional
Cadmium(II) Coordination Polymer Precursor
%V 21
%X A new three-dimensional Cd(II) coordination polymer,
\Cd-3(3-pyc)(4)(NCS)(2)(H2O)(4)center dot 2H(2)O\ (n) (1); 3-Hpyc
= 3-pyridinecarboxylic acid, was prepared and characterized by elemental
analyses and IR spectroscopy. Compound 1 was structurally characterized
by single-crystal X-ray diffraction. The structural determination shows
that the compound is a new 3D coordination polymer has different
environments containing CdO5NS and CdO2N4 units. This polymeric
precursor has been used in the preparation of Cd3OSO4 nanoparticles by
thermolysis in oleic acid. The new nano-structure of Cd3OSO4 was
characterized by scanning electron microscopy and X-ray powder
diffraction. This study demonstrates that coordination polymers may be
suitable precursors to the preparation of desirable nanoscale materials.
@article{ISI:000287249700021,
abstract = {{A new three-dimensional Cd(II) coordination polymer,
\{{[}Cd-3(3-pyc)(4)(NCS)(2)(H2O)(4)]center dot 2H(2)O\} (n) (1); 3-Hpyc
= 3-pyridinecarboxylic acid, was prepared and characterized by elemental
analyses and IR spectroscopy. Compound 1 was structurally characterized
by single-crystal X-ray diffraction. The structural determination shows
that the compound is a new 3D coordination polymer has different
environments containing CdO5NS and CdO2N4 units. This polymeric
precursor has been used in the preparation of Cd3OSO4 nanoparticles by
thermolysis in oleic acid. The new nano-structure of Cd3OSO4 was
characterized by scanning electron microscopy and X-ray powder
diffraction. This study demonstrates that coordination polymers may be
suitable precursors to the preparation of desirable nanoscale materials.}},
added-at = {2017-05-10T15:29:29.000+0200},
address = {{VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS}},
affiliation = {{Shahverdizadeh, GH (Reprint Author), Islamic Azad Univ, Dept Appl Chem, Res Lab, Tabriz Branch, Tabriz, Iran.
Shahverdizadeh, Gholam Hossein, Islamic Azad Univ, Dept Appl Chem, Res Lab, Tabriz Branch, Tabriz, Iran.
Masoudian, Shahla; Soudi, Ali Akbar; Monfared, Hassan Hosseini, Zanjan Univ, Dept Chem, Zanjan, Iran.
Bigdeli, Fahime, Payame Noor Univ, Dept Chem, Abhar, Iran.
Morsali, Ali, Tarbiat Modares Univ, Dept Chem, Fac Sci, Tehran, Iran.
Khavasi, Hamid Reza, Shahid Beheshti Univ, Dept Chem, Tehran, Iran.}},
author = {Shahverdizadeh, Gholam Hossein and Masoudian, Shahla and Soudi, Ali Akbar and Bigdeli, Fahime and Monfared, Hassan Hosseini and Morsali, Ali and Khavasi, Hamid Reza},
author-email = {{Shahverdizadeh@iaut.ac.it
morsali\_a@modares.ac.ir}},
biburl = {https://www.bibsonomy.org/bibtex/250684b6f96af355301cd33c3d14fbb9d/hkhavasi},
cited-references = {{Abu-Youssef MAM, 1999, INORG CHEM, V38, P5716, DOI 10.1021/ic990656x.
AKHBARI K, 2010, COORD CHEM IN PRESS, P254.
Alvarez HM, 2004, POLYHEDRON, V23, P617, DOI 10.1016/j.poly.2003.10.015.
Aoyagi M, 1999, J AM CHEM SOC, V121, P7457, DOI 10.1021/ja991301f.
Ashoka S, 2010, MATER LETT, V64, P173, DOI 10.1016/j.matlet.2009.10.036.
Askanneiad A, 2008, MATER LETT, V62, P478, DOI 10.1016/j.matlet.2007.05.082.
Askarinejad A, 2009, CHEM ENG J, V150, P569, DOI 10.1016/j.cej.2009.03.005.
BUNN AG, 1992, INORG CHEM, V31, P1297, DOI 10.1021/ic00033a031.
Caneschi A, 2001, ANGEW CHEM INT EDIT, V40, P1760, DOI 10.1002/1521-3773(20010504)40:9<1760::AID-ANIE17600>3.0.CO;2-U.
FUJITA M, 1994, J AM CHEM SOC, V116, P1151, DOI 10.1021/ja00082a055.
Janiak C, 1998, J PRAK CHEM-CHEM ZTG, V340, P181, DOI 10.1002/prac.19983400214.
Janiak C, 1998, MAIN GROUP MET CHEM, V21, P33.
Janiak C, 1997, COORDIN CHEM REV, V163, P107, DOI 10.1016/S0010-8545(97)00011-8.
Jayakrishnan R, 2003, THIN SOLID FILMS, V440, P19, DOI 10.1016/S0040-6090(03)00811-3.
LENARVOR N, 1995, J AM CHEM SOC, V117, P7129, DOI 10.1021/ja00132a013.
Mahjoub A, 2003, J COORD CHEM, V56, P779, DOI 10.1080/0095897031000110600.
Mahmoudi G, 2007, CRYSTENGCOMM, V9, P704, DOI 10.1039/b702569f.
Morsali A, 2005, SOLID STATE SCI, V7, P1429, DOI 10.1016/j.solidstatesciences.2005.08.013.
Morsali A, 2005, INORG CHEM COMMUN, V8, P460, DOI 10.1016/j.inoche.2005.02.006.
Morsali A, 2004, INORG CHEM COMMUN, V7, P1184, DOI 10.1016/j.inoche.2004.09.003.
Morsali A, 2009, INORG CHIM ACTA, V362, P3427, DOI 10.1016/j.ica.2009.03.040.
Morsali A, 2009, COORDIN CHEM REV, V253, P1882, DOI 10.1016/j.ccr.2009.02.018.
Nagaraju G, 2009, MATER LETT, V63, P492, DOI 10.1016/j.matlet.2008.11.032.
Nakamoto K., 1997, INFRARED RAMAN SPECT.
Pyykko P, 1997, CHEM REV, V97, P597, DOI 10.1021/cr940396v.
Ristic M, 2004, MATER LETT, V58, P2494, DOI 10.1016/j.matlet.2004.03.016.
Salunkhe RR, 2009, APPL SURF SCI, V255, P3923, DOI 10.1016/j.apsusc.2008.10.035.
Shi WJ, 2007, INORG CHIM ACTA, V360, P588, DOI 10.1016/j.ica.2006.08.004.
Singh N, 2006, MATER LETT, V60, P3492, DOI 10.1016/j.matlet.2006.03.054.
Xiao HP, 2005, HELV CHIM ACTA, V88, P2543, DOI 10.1002/hlca.200590192.}},
doc-delivery-number = {{719ZJ}},
doi = {{10.1007/s10904-010-9443-9}},
funding-acknowledgement = {{Tabriz Azad University}},
funding-text = {{This work was supported by Tabriz Azad University.}},
interhash = {e5cbc992aef4c7deaaa029817cb4c95d},
intrahash = {50684b6f96af355301cd33c3d14fbb9d},
issn = {{1574-1443}},
journal = {{JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS}},
journal-iso = {{J. Inorg. Organomet. Polym. Mater.}},
keywords = {Cadmium(II)} Nano-materials; Thermal properties; structure; {Crystal},
keywords-plus = {{RAY CRYSTAL-STRUCTURE; COMPLEXES; CDO; CHEMISTRY; CD(OH)(2); LIGANDS;
IONS}},
language = {{English}},
month = {{MAR}},
number = {{1}},
number-of-cited-references = {{30}},
orcid-numbers = {{Hosseini-Monfared, Hassan/0000-0001-9157-8198}},
pages = {{171-174}},
publisher = {{SPRINGER}},
research-areas = {{Polymer Science}},
times-cited = {{3}},
timestamp = {2017-05-10T15:29:29.000+0200},
title = {{Direct Synthesis of Cd3OSO4 Nano-particles From a New Three-dimensional
Cadmium(II) Coordination Polymer Precursor}},
type = {{Article}},
unique-id = {{ISI:000287249700021}},
usage-count-last-180-days = {{1}},
usage-count-since-2013 = {{7}},
volume = {{21}},
web-of-science-categories = {{Polymer Science}},
year = {{2011}}
}